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Spectrophotometric determination of bismuth potassium ammonium citrate in cleaning wastes of industrial equipment with 4-(2’-pyridylazo)-resorcinol
https://doi.org/10.26896/1028-6861-2022-88-8-17-26
Аннотация
A simple spectrophotometric method for the determination of bismuth potassium ammonium citrate in the cleaning wastes of industrial equipment using 4-(2’-pyridylazo)-resorcinol is proposed. The method is based on displacement of bismuth from its potassium ammonium citrate by 4-(2’-pyridylazo)-resorcinol, formation of the colored complex, and the colorimetric determination of the resulting product. The calibration curve is linear within the range from 4 to 20 mg/L of bismuth potassium ammonium citrate, the molar attenuation coefficient is 10,100 m2/mol, the detection limit is 2.7 mg/L, the quantification limit is 8.2 mg/L. The method is selective with respect to the common excipients, exhibits a good accuracy (the relative uncertainty does not exceed 10%) and precision (the relative standard deviation does not exceed 5%), does not require lengthy sample preparation and sophisticated laboratory equipment and is suitable for the routine analysis of the cleaning wastes of industrial equipment.
Об авторе
P. A. Nikolaychuk
Chemical Analysis Laboratory, Quality Assurance Department, LLC «Velpharm»
Россия
Россия
Pavel A. Nikolaychuk
11, prosp. Konstitutsii, Kurgan, 640008
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Рецензия
Для цитирования:
Nikolaychuk P.A. Spectrophotometric determination of bismuth potassium ammonium citrate in cleaning wastes of industrial equipment with 4-(2’-pyridylazo)-resorcinol. Заводская лаборатория. Диагностика материалов. 2022;88(8):17-26. https://doi.org/10.26896/1028-6861-2022-88-8-17-26
For citation:
Nikolaychuk P.A. Spectrophotometric determination of bismuth potassium ammonium citrate in cleaning wastes of industrial equipment with 4-(2’-pyridylazo)-resorcinol. Industrial laboratory. Diagnostics of materials. 2022;88(8):17-26. https://doi.org/10.26896/1028-6861-2022-88-8-17-26
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